EXAFS Study of Defect Structure in PbWO4 Single Crystals

FENG Xi-Qi; ZHU Wen-Liang; WU Zong-Hua; XIE Ya-Ning

Chinese Physics C> 2003, Vol. 27> Issue(S1) : 1-4

EXAFS Study of Defect Structure in PbWO4 Single Crystals

The State Key Laboratory of High Performance Ceramics and Superfine Microstructure,Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai 200050,China2 Beijing Synchrotron Laboratory,Institute of High Energy Physics,Chinese Academy of Sciences,Beijing 100039,China

Abstract
HTML
Reference
Related

PDF

Abstract：
The greatly stucture-sensitive characteristic of lead tungstate crystals (PWO) results in a complex defect phenomena inside.This research aims to clarify the mechanism of the annealing process and the doping mechanism of heterovalent ion doping in PWO from a viewpoint of microstructure-analysis.A variety of experiments were performed,including optical absorption spectrospcopy,impedance spectroscopy,X-ray photonelectron spectroscopy and EXAFS anaysis.Among them,EXAFS plays an important role for the availability to provide such structural informations as surrounding species,coordination number,and atomic distance.We report here the results of the defect-investigation in PWO crystals,conducted on the EXAFS experimental station of BSRL in 2002.

References

[1]

HAN Rao-Guo, FENG Xi-Qi et al. J. Appl. Phys. , 1999, 86:3571-35752 Kobayashi M, Usuki Y et al. Nucl. Tnstrum. Meth. Phys. Res.,1997, A399 : 261-2663 HAN Rao-Guo, FENG Xi-Qi et al. J. Appl. Phys. , 1998, 84:2831-28344 LIN Qi-Sheng, FENG Xi-Qi et al. Phys. Rev. B, 2001 , 63: 13415,1-65 Senguttuvan N, lshii M et al. Jpn. J. Appl. Phys. , 2000, 39:5134-51386 SHI Chao-Shu, WET Ya-Guang et al. Chem. Phys. Lett. , 2000,328: 1-47 LIN Qi-Sheng, FENG Xi-Qi. J. Phys. : Condens. Matt. , 2003,15:1963-19738 LI Wen-Sheng, TANG Tong-Rao et al. Jpn. J. Appl. Phys. , 2001 ,40 : 6893-68959 ZHU Wen-Liang, FENG Xi-Qi et al. Phys. Stat. Sol. ( a ) , 2002,193: 211-21610 JAVED M et al. J. Am. Ceram. Sac. , 1975,78: 421-42811 Donnerberg H, Tomlinson S M et al. Phys. Rev. B, 1992,44:4877-4883

[1]	ZHOU Ying-Li , ZHENG Li-Rong , CHU Sheng-Qi , WU Min , AN Peng-Fei , ZHANG Jing , HU Tian-Dou . In-situ EXAFS study on the thermal decomposition of TiH₂. Chinese Physics C, 2014, 38(3): 038001. doi: 10.1088/1674-1137/38/3/038001
[2]	CHU Sheng-Qi , ZHENG Li-Rong , CHE Rong-Zheng , ZHOU Ai-Yu , ZHANG Jing , LIU Jing , HU Tian-Dou . Development of pressure-modulated EXAFS method. Chinese Physics C, 2012, 36(2): 184-187. doi: 10.1088/1674-1137/36/2/015
[3]	SUN Tian-Xi , LIU Zhi-Guo , WEI Shi-Qiang , HE Bo , WEI Zheng , YANG Jun , ZENG Yi , LIN Xiao-Yan , CHU Xue-Lian , DING Xun-Liang . Application of Monolithic Capillary Half Focusing X-Ray Lens in Micro-EXAFS Analytical Technology. Chinese Physics C, 2007, 31(10): 967-971.
[4]	WANG Jia-Ou , DU Yong-Hua , Kurash Ibrahim , HONG Cai-Hao , XIE Ya-Ning , HU Tian-Dou . Study on Perovskite Oxides LaFe_1－xCr_xO₃ by EXAFS. Chinese Physics C, 2007, 31(1): 101-103.
[5]	LIU Lei , CHU Wang-Sheng , ZHONG Jun , MA Si-Xuan , GAO Bin , WU Zi-Yu , GAN Li-Hua , SHU Chun-Ying , WANG Chun-Ru . Preparation and EXAFS Study of Endohedral Metallofulleren Y@C₈₂. Chinese Physics C, 2005, 29(S1): 102-105.
[6]	LIU Miao , QI Ze-Ming , SHI Chao-Shu , XU Mei , ZHANG Wei-Ping , LIU Tao , XIE Ya-Ning . EXAFS Study the Local Structure of Nanocrystalline Lu₂O₃:Eu. Chinese Physics C, 2005, 29(S1): 93-96.
[7]	LI Xian-Liang , PAN Gang , QIN Yan-Wen , HU Tian-Dou , WU Zi-Yu , XIE Ya-Ning , CHEN Hao , DU Yong-Hua . EXAFS Studies on Adsorption Microscopic Structures of Zn at Manganite-Water Interaface and δ-MnO₂-Water Interaface. Chinese Physics C, 2003, 27(S1): 23-27.
[8]	LIANG Ling , GU Mu , DUAN Yong , MA Xiao-Hui , LIU Feng-Song , WU Xiang-Hui , QIU Long-Qing , CHEN Ming-Nan , LIAO Jing-Ying , SHEN Ding-Zhong , ZHANG Xin , GONG Bo , XUE Xuan-Ping , , . Study on Irradiation Damage of Bi-Doped PbWO₄ Crystal. Chinese Physics C, 2003, 27(6): 526-531.
[9]	YUAN Qing-Xi , XU Jun , PAN Shou-Kui , HUANG Wan-Xia , TIAN Yu-Lian , JIANG Jian-Hua . In Situ Observation of Domain Structure of Molybdates Gadolinum Single Crystal by Synchrotron X-Ray Topography. Chinese Physics C, 2001, 25(S1): 116-120.
[10]	YU Wan-Li , LUO Yong-An , WANG Ming-Zhi , ZHENG Qiu-Ju , ZHANG Hui-Jun , TIAN Yu-Lian , HUANG Wan-Xia . A New Method to Determine the Orientations of Crystal Defects by Synchrotron Radiation. Chinese Physics C, 2001, 25(S1): 110-115.
[11]	YANG Peng-Cheng , CAI Xiao-Hai , HAO Jun-Chang , ZI Feng-Lan , XIE You-Chang , HU Tian-Dou , XIE Ya-Ning , ZHANG Jing . EXAFS Study of ZnO/γ-Al₂O₃ Prepared by Co-Precipitation Method. Chinese Physics C, 2001, 25(S1): 17-20.
[12]	SHAO Ming , LIU Yan-Wen , ZHANG Zi-Ping , CHEN Hong-Fang . Study on Light Collection Uniformity of Long Lead Tungstate Crystal by Monte Carlo Method. Chinese Physics C, 2001, 25(1): 50-56.
[13]	SHAO Ming , CHEN HongFang , LI Cheng , CHEN Hui , XU ZiZong , WANG ZhaoMin . Testing the Radiation Hardness of Lead Tungstate Scintilating Crystals. Chinese Physics C, 2000, 24(6): 554-559.
[14]	Wu Chong , Li Cheng , Wang Zhaomin , Gong Zhufang , Chen Hongfang , Xu Zizong , Liao Jingying , Yuan Hin . Measurement of Properties of Lead Tungstates. Chinese Physics C, 1999, 23(12): 1141-1147.
[15]	Li Zuhao , He Jingtang , Lu Yusheng , Chen Duanbao , Bian Jianguo , Zhu Guoyi , Tang Xiaowei . Study on Radiation Damage of Lead Tungstate Crystals. Chinese Physics C, 1999, 23(12): 1148-1151.
[16]	GU Yi-Fan , HE Jing-Tang , QIAN Zhong-Min , ZHU Guo-Yi , XU Yu-Heng , WAN Li-De , CHEN Gang , HE Zheng-Shu . A STUDY OF THE PROPERTIES OF ZINC TUNGSTATE FOR DETECTION OF PHOTONS. Chinese Physics C, 1988, 12(5): 577-580.
[17]	GU Yi-Fan , HE Jing-Tang , WANG Mao-Zi , ZHU Guo-Yi , YE Zong-Yuan , YUAN Guan-Jun , YU Pan-Shui , YANG Chun-Xiang . THE RESPONSE OF A 3×3 BGO DETECTOR ARRAY TO 0.5—21MeV PHOTONS. Chinese Physics C, 1987, 11(1): 16-23.
[18]	XIONG Xing-Min . A STUDY OF DEFECTS DEFECTS IN GaAs BY POSITRON ANNIHILATION. Chinese Physics C, 1986, 10(4): 459-465.
[19]	FANG Bao , XIA Ke-Ding , FU De-Ji , XU Gong-Ou . THE STUDY OF QUADRUPOLE MOMENT, OCTUPOLE TRANSITION AND TRANSITION DENSITY OF ²⁰⁸Pb 3^－STATE—— THE APPLICATION OF GENERATOR COORDINATE METHOD (GCM). Chinese Physics C, 1984, 8(4): 461-469.
[20]	HE JING-TANG , GU YI-FAN , SHEN BING-FU , . A STUDY OF THE PROPERTIES OF BISMUTH GERMANATE FOR DETECTION OF PHOTONS. Chinese Physics C, 1983, 7(6): 766-771.

Access

Get Citation

FENG Xi-Qi, ZHU Wen-Liang, WU Zong-Hua and XIE Ya-Ning. EXAFS Study of Defect Structure in PbWO4 Single Crystals[J]. Chinese Physics C, 2003, 27(S1): 1-4.

FENG Xi-Qi, ZHU Wen-Liang, WU Zong-Hua and XIE Ya-Ning. EXAFS Study of Defect Structure in PbWO4 Single Crystals[J]. Chinese Physics C, 2003, 27(S1): 1-4. shu

RIS(for EndNote,Reference Manager,ProCite)

BibTex

Txt

Milestone

Received: 2003-11-21
Revised: 1900-01-01

Article Metric

Article Views(4138)
PDF Downloads(1114)
Cited by(0)

Policy on re-use

To reuse of subscription content published by CPC, the users need to request permission from CPC, unless the content was published under an Open Access license which automatically permits that type of reuse.

通讯作者: 陈斌, bchen63@163.com

1.
沈阳化工大学材料科学与工程学院沈阳 110142

EXAFS Study of Defect Structure in PbWO4 Single Crystals

Corresponding author: FENG Xi-Qi,

The State Key Laboratory of High Performance Ceramics and Superfine Microstructure,Shanghai Institute of Ceramics,Chinese Academy of Sciences,Shanghai 200050,China2 Beijing Synchrotron Laboratory,Institute of High Energy Physics,Chinese Academy of Sciences,Beijing 100039,China

Received Date: 2003-11-21

Accepted Date: 1900-01-01

Available Online: 2003-01-02

Abstract: The greatly stucture-sensitive characteristic of lead tungstate crystals (PWO) results in a complex defect phenomena inside.This research aims to clarify the mechanism of the annealing process and the doping mechanism of heterovalent ion doping in PWO from a viewpoint of microstructure-analysis.A variety of experiments were performed,including optical absorption spectrospcopy,impedance spectroscopy,X-ray photonelectron spectroscopy and EXAFS anaysis.Among them,EXAFS plays an important role for the availability to provide such structural informations as surrounding species,coordination number,and atomic distance.We report here the results of the defect-investigation in PWO crystals,conducted on the EXAFS experimental station of BSRL in 2002.

HTML

Reference (1)

EXAFS Study of Defect Structure in PbWO4 Single Crystals

Abstract：

References

Access

Article Metrics

Metrics

通讯作者: 陈斌, bchen63@163.com

Email This Article